Characterization of transmission volume holographic gratings recorded in Slavich PFG04 dichromated gelatin plates

Ayalid Villamarín; Jesús Atencia; M. Victoria Collados; Manuel Quintanilla

doi:10.1364/AO.48.004348

Applied Optics
Vol. 48,
Issue 22,
pp. 4348-4353
(2009)
•https://doi.org/10.1364/AO.48.004348

Characterization of transmission volume holographic gratings recorded in Slavich PFG04 dichromated gelatin plates

Ayalid Villamarín, Jesús Atencia, M. Victoria Collados, and Manuel Quintanilla

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Ayalid Villamarín, Jesús Atencia, M. Victoria Collados, and Manuel Quintanilla, "Characterization of transmission volume holographic gratings recorded in Slavich PFG04 dichromated gelatin plates," Appl. Opt. 48, 4348-4353 (2009)

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Abstract

We characterize Slavich PFG-04 dichromated gelatin plates to make transmission volume holographic elements recorded with a $532 nm$ laser source, obtaining high efficiency gratings with a high signal to noise ratio. The linear dynamic range of the material is studied by measuring the efficiency of multiplexed gratings. Results obtained are applied to the recording of holographic elements with high efficiency when they are illuminated with a $800 nm$ light source.

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Index Matching Liquid	Refractive Index ( $λ_{D} = 589.3 nm$ , $20 ° C$ )	Effects on Emulsion
Glycerol	1.4740	Reacts with dichromate
Glycerol triacetate	1.4310	The emulsion is detached from the glass substrate
Immersion oil for microscopy purposes (Panreac)	1.517	The emulsion is detached from the glass substrate
Benzyl alcohol	1.5396	The emulsion is detached from the glass substrate
Xylene	1.5058	The emulsion is detached from the glass substrate
Tetrachloroethylene	1.5056	The emulsion is detached from the glass substrate
Acetone	1.3591	The emulsion is detached from the glass substrate
BK7 Immersion oil (Cargille)	1.5167	Compatible
Baby oil (Johnson’s)	1.4671	Compatible
B-oil for rotatory vane purposes	1.4736	The emulsion is detached from the glass substrate
Quintanilla index matching liquid [25] (80% benzyl alcohol and 20% glycerol triacetate)	1.5142 ( $λ = 632.8 nm$ )	The emulsion is detached from the glass substrate

Process	Time (min)	Agent	Temperature $° C$
Thermal hardening	^a	Forced air oven	100
Washing and swelling	4	Filtered current water	20
Swelling	3	Distilled water	20
Dehydration	3	$Isopropyl alcohol + water$ ( $50 ∶ 50$ )	20
Dehydration	3	$Isopropyl alcohol + water$ ( $75 ∶ 25$ )	20
Dehydration	3	Isopropyl alcohol 100%	20
Dried	60	Forced air oven	100

Index Matching Liquid	Refractive Index ( $λ_{D} = 589.3 nm$ , $20 ° C$ )	Effects on Emulsion
Glycerol	1.4740	Reacts with dichromate
Glycerol triacetate	1.4310	The emulsion is detached from the glass substrate
Immersion oil for microscopy purposes (Panreac)	1.517	The emulsion is detached from the glass substrate
Benzyl alcohol	1.5396	The emulsion is detached from the glass substrate
Xylene	1.5058	The emulsion is detached from the glass substrate
Tetrachloroethylene	1.5056	The emulsion is detached from the glass substrate
Acetone	1.3591	The emulsion is detached from the glass substrate
BK7 Immersion oil (Cargille)	1.5167	Compatible
Baby oil (Johnson’s)	1.4671	Compatible
B-oil for rotatory vane purposes	1.4736	The emulsion is detached from the glass substrate
Quintanilla index matching liquid [25] (80% benzyl alcohol and 20% glycerol triacetate)	1.5142 ( $λ = 632.8 nm$ )	The emulsion is detached from the glass substrate

Process	Time (min)	Agent	Temperature $° C$
Thermal hardening	^a	Forced air oven	100
Washing and swelling	4	Filtered current water	20
Swelling	3	Distilled water	20
Dehydration	3	$Isopropyl alcohol + water$ ( $50 ∶ 50$ )	20
Dehydration	3	$Isopropyl alcohol + water$ ( $75 ∶ 25$ )	20
Dehydration	3	Isopropyl alcohol 100%	20
Dried	60	Forced air oven	100

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Applied Optics