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Applied Optics

Applied Optics


  • Vol. 43, Iss. 13 — May. 1, 2004
  • pp: 2792–2797

Parametric study of pellets for elemental analysis with laser-induced breakdown spectroscopy

Bansi Lal, Hongbo Zheng, Fang-Yu Yueh, and Jagdish P. Singh  »View Author Affiliations

Applied Optics, Vol. 43, Issue 13, pp. 2792-2797 (2004)

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The effect of various parameters on the accuracy of the laser-induced breakdown spectroscopy (LIBS) data taken from pellet samples has been investigated. The dependence of the standard deviation of the LIBS data on the amount and nature of the binder used, pressure used to press the powder into a pellet, and the position of the focal spot on the pellet has been investigated. Pellets made from industrially important materials such as silica, alumina, and lime with polyvinyl alcohol, sucrose, and starch as binders have been studied. The results thus obtained are tested by preparation of the calibration curves for Si, Fe, and B in the pellets made from the powder glass batch used as a surrogate for the batch employed for the vitrification of radioactive waste.

© 2004 Optical Society of America

OCIS Codes
(120.6200) Instrumentation, measurement, and metrology : Spectrometers and spectroscopic instrumentation
(140.3440) Lasers and laser optics : Laser-induced breakdown
(300.2140) Spectroscopy : Emission
(300.6210) Spectroscopy : Spectroscopy, atomic

Original Manuscript: July 2, 2003
Revised Manuscript: December 15, 2003
Published: May 1, 2004

Bansi Lal, Hongbo Zheng, Fang-Yu Yueh, and Jagdish P. Singh, "Parametric study of pellets for elemental analysis with laser-induced breakdown spectroscopy," Appl. Opt. 43, 2792-2797 (2004)

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