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Optica Publishing Group
  • Applied Spectroscopy
  • Vol. 52,
  • Issue 2,
  • pp. 205-211
  • (1998)

Reducing Polyatomic Interferences in the ICP-MS Determination of Chromium and Vanadium in Biofluids and Tissues

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Abstract

The suitability of inductively coupled plasma quadrupole mass spectrometry (ICP-MS) for the determination of Cr and V in biofluids and tissues has been studied. High-pressure thermal and moderatepressure microwave sample preparation with vapor-phase acid digestion successfully minimized blanks and carbon and chloride interferences. The remaining ArC 1 interferences on 52Cr were corrected mathematically. Analysis of standard reference materials verified the accuracy of the method.

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