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Optica Publishing Group
  • Applied Spectroscopy
  • Vol. 10,
  • Issue 4,
  • pp. 193-194
  • (1956)

A Direct Infrared Method for Determining 4-Methyl-2,6-Ditertiarybutylphenol in Mineral Oil

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Abstract

A conventent and rapid direct infrared method for determining 4-methyl-2,6-ditertiarybutylphenol in mineral oil has been developed that uses the 2.74-micron hydroxyl band. The spectrum of the sample is recorded between 2.65 and 2.85 microns to obtain a pair of absorbances from which the phenol concentration is determined. The corresponding phenol-free oil is not needed, and no sample preparation is required when other substances containing the hydroxyl group are absent. The method is accurate to 0.01% phenol; instrument time is about five minutes.

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