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Applied Spectroscopy

Applied Spectroscopy

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  • Vol. 11, Iss. 4 — Nov. 1, 1957
  • pp: 188–189

Deuteration of Acrylonitrile

W. F. Cockburn and C. E. Hubley

Applied Spectroscopy, Vol. 11, Issue 4, pp. 188-189 (1957)


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Abstract

During preparation of acrylonitrile-1-d, CH2=CHD—CN, by D2O exchange, as described by Leitch (1), it was found that a linear relationship obtained between absorbance values for the 1165 cm−1 band and the degree of exchange indicated by mass spectrometer data. This note contains a brief description of the exchange experiment, spectra of acrylonitrile before and after deuteration, and a table of IR and mass spectral data recorded at intervals during the exchange.

Citation
W. F. Cockburn and C. E. Hubley, "Deuteration of Acrylonitrile," Appl. Spectrosc. 11, 188-189 (1957)
http://www.opticsinfobase.org/as/abstract.cfm?URI=as-11-4-188

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