OSA's Digital Library

Applied Spectroscopy

Applied Spectroscopy

| PUBLISHED BY SAS — AVAILABLE FROM SAS AND OSA

  • Vol. 23, Iss. 4 — Jul. 1, 1969
  • pp: 376–377

An Improved Technique for Handling Milligram Samples for Nuclear Magnetic Resonance Analysis

David W. Mastbrook and Edward P. Ragelis

Applied Spectroscopy, Vol. 23, Issue 4, pp. 376-377 (1969)


View Full Text Article

Acrobat PDF (175 KB)





Browse Journals / Lookup Meetings

Browse by Journal and Year


   


Lookup Conference Papers

Close Browse Journals / Lookup Meetings

Article Tools

Share
Citations
  • Export Citation/Save Click for help

Abstract

We have been handling milligram samples for nuclear magnetic resonance (NMR) spectroscopy in a capillary with a technique that was developed mainly with gas–liquid chromatography (GLC) collection in mind; however, this technique can also be applied when the sample capillary is filled by a syringe or capillary action. The technique compares favorably with similar ones reported, and combines the following advantages: (1) There is greater flexibility as to the amount of sample collected by GLC. (2) No transfer of the sample from the GLC collection tube to the NMR tube is necessary. (3) Filling and positioning of the collection tube in the probe is less cumbersome than with other microcells. (4) All components are commercially available at low cost and can be assembled quickly.

Citation
David W. Mastbrook and Edward P. Ragelis, "An Improved Technique for Handling Milligram Samples for Nuclear Magnetic Resonance Analysis," Appl. Spectrosc. 23, 376-377 (1969)
http://www.opticsinfobase.org/as/abstract.cfm?URI=as-23-4-376


Sort:  Journal  |  Reset

References

References are not available for this paper.

Cited By

OSA is able to provide readers links to articles that cite this paper by participating in CrossRef's Cited-By Linking service. CrossRef includes content from more than 3000 publishers and societies. In addition to listing OSA journal articles that cite this paper, citing articles from other participating publishers will also be listed.

« Previous Article  |  Next Article »

OSA is a member of CrossRef.

CrossCheck Deposited