OSA's Digital Library

Applied Spectroscopy

Applied Spectroscopy

| PUBLISHED BY SAS — AVAILABLE FROM SAS AND OSA

  • Vol. 40, Iss. 5 — Jul. 1, 1986
  • pp: 673–680

Continuous, On-Line Interface for Reverse-Phase Microbore High-Performance Liquid Chromatography/Diffuse Reflectance Infrared Fourier Transform Analysis

M. A. Castles, L. V. Azarraga, and L. A. Carreira

Applied Spectroscopy, Vol. 40, Issue 5, pp. 673-680 (1986)


View Full Text Article

Acrobat PDF (792 KB)





Browse Journals / Lookup Meetings

Browse by Journal and Year


   


Lookup Conference Papers

Close Browse Journals / Lookup Meetings

Article Tools

Share
Citations
  • Export Citation/Save Click for help

Abstract

An ultrasonic nebulizer with a piezo-electric transducer and a newly designed and constructed continuous on-line collection station have been adapted as an interface between a reverse-phase microbore high-performance liquid chromatograph (RP-μHPLC) and a diffuse reflectance infrared Fourier transform spectrometer. The collection station incorporates a directional vacuum port for confinement of the nebulized material onto a small area (3 to 5 mm i.d.) of the diamond powder. The inherent desolvation that occurs upon nebulization of the reverse-phase eluant, along with the vacuum collection system and the diamond powder diffuse reflectance substrate, makes possible the continuous on-line collection and FT-IR analysis of the compounds separated by a RP-μHPLC without any type of initial solute extraction.

Citation
M. A. Castles, L. V. Azarraga, and L. A. Carreira, "Continuous, On-Line Interface for Reverse-Phase Microbore High-Performance Liquid Chromatography/Diffuse Reflectance Infrared Fourier Transform Analysis," Appl. Spectrosc. 40, 673-680 (1986)
http://www.opticsinfobase.org/as/abstract.cfm?URI=as-40-5-673

You do not have subscription access to this journal. Citation lists with outbound citation links are available to subscribers only. You may subscribe either as an OSA member, or as an authorized user of your institution.

Contact your librarian or system administrator
or
Log in to access OSA Member Subscription

You do not have subscription access to this journal. Cited by links are available to subscribers only. You may subscribe either as an OSA member, or as an authorized user of your institution.

Contact your librarian or system administrator
or
Log in to access OSA Member Subscription

« Previous Article  |  Next Article »

OSA is a member of CrossRef.

CrossCheck Deposited