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Applied Spectroscopy

Applied Spectroscopy

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  • Vol. 43, Iss. 7 — Sep. 1, 1989
  • pp: 1168–1172

Simultaneous Detection of Optical Isomers and the Separation of Overlapping Resonances in a 1H NMR Spectrum of (+/-)-2,2-Dimethyl-1-Phenyl-1-Propanol Using an NMR Shift Reagent

Ashok L. Cholli and Miu-Ling Lau

Applied Spectroscopy, Vol. 43, Issue 7, pp. 1168-1172 (1989)


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Abstract

The enantiomer separation and the spectral simplification of overlapped resonances in a high-resolution 1H NMR spectrum of a model compound have been successfully accomplished with the use of paramagnetic shift reagent. Both 1H and 13C NMR have been applied to determine the composition of a mixture containing optically active enantiomers of (+/-)-2,2-dimethyl-1-phenyl-1-propanol.

Citation
Ashok L. Cholli and Miu-Ling Lau, "Simultaneous Detection of Optical Isomers and the Separation of Overlapping Resonances in a 1H NMR Spectrum of (+/-)-2,2-Dimethyl-1-Phenyl-1-Propanol Using an NMR Shift Reagent," Appl. Spectrosc. 43, 1168-1172 (1989)
http://www.opticsinfobase.org/as/abstract.cfm?URI=as-43-7-1168


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