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Applied Spectroscopy

Applied Spectroscopy

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  • Vol. 51, Iss. 7 — Jul. 1, 1997
  • pp: 1042–1046

Depth Profiling of Thick Layers of Graded Metal-Zirconia Ceramic Coatings Using Laser Ablation Inductively Coupled Plasma Atomic Emission Spectrometry

Viktor Kanicky, Ivan Novotny, Jan Musil, and Jean-Michel Mermet

Applied Spectroscopy, Vol. 51, Issue 7, pp. 1042-1046 (1997)


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Abstract

The feasibility of depth profiling of thick layers ( > 100 mu m) consisting of partially stabilized zirconia coating and graded metal-ceramic coating on Inconel steel (ZrO2-Y2O3 /NiCrAlY/steel and ZrO2 CeO2/NiCrAlY/steel) was studied on the basis of the use of laser ablation inductively coupled plasma atomic emission spectrometry (LA-ICP-AES). An ICP spectrometer equipped with a multichannel detection was used for the simultaneous measurements of the line intensities. The ablation was performed with a Nd:YAG laser operated in a Q-switched mode at 266 nm. To study the erosion rate, we used either a static or a translation mode for the ablation, and the corresponding temporal behavior of the signals was studied. A higher erosion rate was found for the translation mode when depths higher than several hundred micrometers were probed.

Citation
Viktor Kanicky, Ivan Novotny, Jan Musil, and Jean-Michel Mermet, "Depth Profiling of Thick Layers of Graded Metal-Zirconia Ceramic Coatings Using Laser Ablation Inductively Coupled Plasma Atomic Emission Spectrometry," Appl. Spectrosc. 51, 1042-1046 (1997)
http://www.opticsinfobase.org/as/abstract.cfm?URI=as-51-7-1042


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