Abstract

The thermal decompositions of [MoO₃(2,2'-bipy)], [Mo₂O₆(2,2'-bipy)], and [Mo₃O₉(2,2'-bipy)₂] have been studied by Raman spectroscopy. Upon heating, [MoO₃(2,2'-bipy)] loses 2,2'-bipyridine and converts to MoO₃ through a stable intermediate, [Mo₂O₆(2,2'-bipy)], whereas [Mo₃O₉(2,2'-bipy)₂] loses 2,2'-bipyridine and transforms to MoO₃directly. Vibrational assignments for [MoO₃(2,2'-bipy)], [Mo₂O₆(2,2'-bipy)], and [Mo₃O₉(2,2'-bipy)₂] are proposed.

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