OSA's Digital Library

Journal of the Optical Society of America

Journal of the Optical Society of America

  • Vol. 55, Iss. 2 — Feb. 1, 1965
  • pp: 133–135

New Cryogenic Method for Raman Studies of Molecular Crystals

R. SAVOIE and A. ANDERSON  »View Author Affiliations


JOSA, Vol. 55, Issue 2, pp. 133-135 (1965)
http://dx.doi.org/10.1364/JOSA.55.000133


View Full Text Article

Acrobat PDF (347 KB)





Browse Journals / Lookup Meetings

Browse by Journal and Year


   


Lookup Conference Papers

Close Browse Journals / Lookup Meetings

Article Tools

Share
Citations

Abstract

A new technique has been developed for growing good quality molecular crystals, suitable for Raman studies at low temperatures. The method utilizes a copper rod, cooled by a suitable refrigerant, which lies axially in the sample tube. The crystal grows radially around the rod from the melt. Liquid nitrogen and helium cryostats, incorporating this method, for use with the Cary 81 spectrophotometer, are described. These can be readily modified to suit other Raman instruments. Low Rayleigh scattering near the exciting line and the very sharp spectral lines of a number of samples so far studied indicate the good quality of such crystals, grown in a relatively short time.

Citation
R. SAVOIE and A. ANDERSON, "New Cryogenic Method for Raman Studies of Molecular Crystals," J. Opt. Soc. Am. 55, 133-135 (1965)
http://www.opticsinfobase.org/josa/abstract.cfm?URI=josa-55-2-133


Sort:  Author  |  Journal  |  Reset

References

  1. For bibliography, see W. Vedder and D. F. Hornig, Advan. Spectry. 2, 189 (1961).
  2. D. F. Hornig, J. Chem. Phys. 16, 1003 (1948).
  3. H. Winston and R. S. Halford, J. Chem. Phys. 17, 607 (1949).
  4. D. W. Robinson, "Pittsburgh Conference on Analytical Chemistry and Applied Spectroscopy," paper No. 104 (1964).
  5. S. H. Walmsley and A. Anderson, Mol. Phys. 7, 401, 411 (1964).
  6. G. B. B. M. Sutherland and Cheng-Kai Wu, Proc. Roy. Soc. (London) A176, 491 (1940).
  7. F. P. Reding and D. F. Hornig, J. Chem. Phys. 22, 1926 (1954).
  8. W. J. Taylor, L. Smith, and H. L. Johnston, J. Opt. Soc. Am. 41, 91 (1951).
  9. J. R. Ferraro, J. S. Ziomek, and K. Puckett, Rev. Sci. Instr. 35, 754 (1964).
  10. S. S. Bhatnagar, E. J. Allin, and H. L. Welsh, Can. J. Phys. 9 (1962).
  11. Suitable seals are obtainable from the Carborundum Company.
  12. Preliminary report: R. Savoie and A. Anderson, "Columbus Symposium on Molecular Structure and Spectroscopy," Paper No. C8 (1964).

Cited By

Alert me when this paper is cited

OSA is able to provide readers links to articles that cite this paper by participating in CrossRef's Cited-By Linking service. CrossRef includes content from more than 3000 publishers and societies. In addition to listing OSA journal articles that cite this paper, citing articles from other participating publishers will also be listed.

« Previous Article  |  Next Article »

OSA is a member of CrossRef.

CrossCheck Deposited