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Optics Express

Optics Express

  • Editor: C. Martijn de Sterke
  • Vol. 20, Iss. 4 — Feb. 13, 2012
  • pp: 4039–4049

Three-dimensional structure of a single colloidal crystal grain studied by coherent x-ray diffraction

J. Gulden, O. M. Yefanov, A. P. Mancuso, R. Dronyak, A. Singer, V. Bernátová, A. Burkhardt, O. Polozhentsev, A. Soldatov, M. Sprung, and I. A. Vartanyants  »View Author Affiliations


Optics Express, Vol. 20, Issue 4, pp. 4039-4049 (2012)
http://dx.doi.org/10.1364/OE.20.004039


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Abstract

A coherent x-ray diffraction experiment was performed on an isolated colloidal crystal grain at the coherence beamline P10 at PETRA III. Using azimuthal rotation scans the three-dimensional (3D) scattered intensity from the sample in the far-field was measured. It includes several Bragg peaks as well as the coherent interference around these peaks. The analysis of the scattered intensity reveals the presence of plane defects in a single grain of the colloidal sample. We confirm these findings by model simulations. In these simulations we also analyze the experimental conditions required to phase the 3D diffraction pattern from a single colloidal grain. This approach has the potential to produce a high resolution image of the sample revealing its inner structure, with possible structural defects.

© 2012 OSA

OCIS Codes
(050.1940) Diffraction and gratings : Diffraction
(100.5070) Image processing : Phase retrieval
(340.7460) X-ray optics : X-ray microscopy
(160.5298) Materials : Photonic crystals

ToC Category:
X-ray Optics

History
Original Manuscript: December 15, 2011
Revised Manuscript: January 20, 2012
Manuscript Accepted: January 20, 2012
Published: February 2, 2012

Citation
J. Gulden, O. M. Yefanov, A. P. Mancuso, R. Dronyak, A. Singer, V. Bernátová, A. Burkhardt, O. Polozhentsev, A. Soldatov, M. Sprung, and I. A. Vartanyants, "Three-dimensional structure of a single colloidal crystal grain studied by coherent x-ray diffraction," Opt. Express 20, 4039-4049 (2012)
http://www.opticsinfobase.org/oe/abstract.cfm?URI=oe-20-4-4039


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