OSA's Digital Library

Optics Express

Optics Express

  • Editor: Michael Duncan
  • Vol. 12, Iss. 6 — Mar. 22, 2004
  • pp: 1055–1060

Characterization of surface crystallization in Ge-doped graded-index silica glass

Honglin An, Ying Tang, Pam McNamara, and Simon Fleming  »View Author Affiliations


Optics Express, Vol. 12, Issue 6, pp. 1055-1060 (2004)
http://dx.doi.org/10.1364/OPEX.12.001055


View Full Text Article

Enhanced HTML    Acrobat PDF (1599 KB)





Browse Journals / Lookup Meetings

Browse by Journal and Year


   


Lookup Conference Papers

Close Browse Journals / Lookup Meetings

Article Tools

Share
Citations

Abstract

Surface crystallization was induced in Ge-doped silica glass samples from a graded-index optical fiber preform by re-heating them at 1100°C for several hours. X-ray diffraction and second-harmonic generation (SHG) microscopy have been utilized to investigate the crystalline phases formed. Experimental results indicate that the predominant crystalline phase is α-cristobalite. The cross-sectional distribution of the crystal particles has also been measured with the SHG microscopy and the result is in good agreement with that from traditional bright field light microscopy.

© 2004 Optical Society of America

OCIS Codes
(160.2750) Materials : Glass and other amorphous materials
(190.1900) Nonlinear optics : Diagnostic applications of nonlinear optics
(190.4400) Nonlinear optics : Nonlinear optics, materials

ToC Category:
Research Papers

History
Original Manuscript: February 11, 2004
Revised Manuscript: February 29, 2004
Published: March 22, 2004

Citation
Honglin An, Ying Tang, Pam McNamara, and Simon Fleming, "Characterization of surface crystallization in Ge-doped graded-index silica glass," Opt. Express 12, 1055-1060 (2004)
http://www.opticsinfobase.org/oe/abstract.cfm?URI=oe-12-6-1055


Sort:  Journal  |  Reset  

References

  1. P. M. McMillan, Glass-ceramics (Academic, 1964), Chap. 4.
  2. A. Narazaki, K. Tanaka, and K. Hirao, �??Optical second-order nonlinearity of transparent glass-ceramics containing BaTiO3 precipitated via surface crystallization,�?? J. Mater. Res. 14, 3640-3646 (1999). [CrossRef]
  3. Y. Takahashi, Y. Benino, T. Fujiwara, and T. Komatsu, �??Second harmonic generation in transparent surface crystallized glasses with stillwellite-type LaBGeO5,�?? J. Appl. Phys. 89, 5282-5287 (2001). [CrossRef]
  4. T. Fujiwara, H. Nagata, Y. Benino, and T. Komatsu, �??Crystallization behaviors with pre-treatments of thermal annealing and ultraviolet laser irradiation in Ge-doped SiO2 glass fiber preforms,�?? J. Ceram. Soc. Jpn. 111, 8-10 (2003). [CrossRef]
  5. T. Fujiwara, T. Sawada, Y. Benino, T. Komatsu, M. Takahashi, T. Yoko, and J. Nishii, �??Direct observation of second-harmonic generation from crystalline particles in Ge-doped SiO2 glass films,�?? Opt. Express 11, 1598 (2003), <a href="http://www.opticsexpress.org/abstract.cfm?URI=OPEX-11-14-1598.">http://www.opticsexpress.org/abstract.cfm?URI=OPEX-11-14-1598</a> [CrossRef] [PubMed]
  6. Y. Uesu, S. Kurimura, and Y. Yamamoto, �??Optical second harmonic images of 90° domain structure in BaTiO3 and periodically inverted antiparallel domains in LiTaO3,�?? Appl. Phys. Lett. 66, 2165-2167 (1995). [CrossRef]
  7. D. M. Hatch and S. Ghose, �??The alpha-beta phase-transition in cristobalite, SiO2 - symmetry analysis, domain-structure, and the dynamic nature of the beta-phase,�?? Phys. Chem. Miner. 17, 554-562 (1991). [CrossRef]
  8. C. H. Chao and H. Y. Lu, �??Stress-induced β�??α-cristobalite phase transformation in (Na2O+Al2O3)-codoped silica,�?? Mater. Sci. Eng. A328, 267-276 (2002).
  9. C. Cabrillo, F.J. Bermejo, J.M. Gibson, J.A. Johnson, D. Faccio, V. Pruneri, and P.G. Kazansky, �??Thermally poled silica samples are structurally heterogeneous: Electron diffraction evidence of partial crystallization,�?? Appl. Phys. Lett. 78, 1991-1993 (2001). [CrossRef]

Cited By

Alert me when this paper is cited

OSA is able to provide readers links to articles that cite this paper by participating in CrossRef's Cited-By Linking service. CrossRef includes content from more than 3000 publishers and societies. In addition to listing OSA journal articles that cite this paper, citing articles from other participating publishers will also be listed.


« Previous Article  |  Next Article »

OSA is a member of CrossRef.

CrossCheck Deposited