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Optical absorption of two dimensional periodic microstructures on ZnO crystal fabricated by the interference of two femtosecond laser beamsXin Jia, Tianqing Jia, Yi Zhang, Pingxin Xiong, Donghai Feng, Zhenrong Sun, and Zhizhan Xu »View Author Affiliations
Xin Jia,
Tianqing Jia,*
Yi Zhang,
Pingxin Xiong,
Donghai Feng,
Zhenrong Sun,1
and Zhizhan Xu2
1State Key Laboratory of Precision Spectroscopy, Department of Physics, East China Normal University, Shanghai 200062, P. R. China 1zrsun@phy.ecnu.edu.cn 2zzxu@mail.shcnc.ac.cn *Corresponding author: tqjia@phy.ecnu.edu.cn |
Optics Express, Vol. 18, Issue 14, pp. 14401-14408 (2010)
http://dx.doi.org/10.1364/OE.18.014401
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Abstract
Two dimensional (2D) periodic microstructures composed of short periodic ripples, long periodic ripples and micro-holes are fabricated on ZnO crystals via the interference of two femtosecond laser beams. The relative reflectivity and transmissivity of visible light of these 2D microstructures decrease to the values of 30% and 20%, respectively. Theoretical and experimental studies indicate that besides the effects of increased surface area, the decrease of reflectivity is influenced greatly by the Mie scattering of surface microstructures, and the transmissivity, by the damage of crystalline structures.
© 2010 OSA
OCIS Codes
(220.4000) Optical design and fabrication : Microstructure fabrication
(320.7130) Ultrafast optics : Ultrafast processes in condensed matter, including semiconductors
ToC Category:
Laser Microfabrication
History
Original Manuscript: May 24, 2010
Manuscript Accepted: May 31, 2010
Published: June 21, 2010
Citation
Xin Jia, Tianqing Jia, Yi Zhang, Pingxin Xiong, Donghai Feng, Zhenrong Sun, and Zhizhan Xu, "Optical absorption of two dimensional periodic microstructures on ZnO crystal fabricated by the interference of two femtosecond laser beams," Opt. Express 18, 14401-14408 (2010)
http://www.opticsinfobase.org/oe/abstract.cfm?URI=oe-18-14-14401
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References
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- X. D. Guo, R. X. Li, Y. Hang, Z. Z. Xu, B. K. Yu, H. L. Ma, and X. W. Sun, “Raman spectroscopy and luminescent properties of ZnO nanostructures fabricated by femtosecond laser pulses,” Mater. Lett. 61(23-24), 4583–4586 (2007). [CrossRef]
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- X. D. Guo, R. X. Li, Y. Hang, Z. Z. Xu, B. K. Yu, H. L. Ma, and X. W. Sun, “Raman spectroscopy and luminescent properties of ZnO nanostructures fabricated by femtosecond laser pulses,” Mater. Lett. 61(23-24), 4583–4586 (2007). [CrossRef]
- E. Hsu, T. Crawford, C. Maunders, G. Botton, and H. Haugen, “Cross-sectional study of periodic surface structures on gallium phosphide induced by ultrashort laser pulse irradiation,” Appl. Phys. Lett. 92(22), 221112 (2008). [CrossRef]
- T. Q. Jia, H. X. Chen, M. Huang, F. L. Zhao, X. X. Li,, S. Z. Xu, H. Y. Sun, D. H. Feng, C. B. Li, X. F. Wang, R. X. Li, Z. Z. Xu, X. K. He, and H. Kuroda, “Ultraviolet-infrared femtosecond laser-induced damage in fused silica and CaF2 crystals,” Phys. Rev. B 73(5), 054105 (2006). [CrossRef]
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- V. R. Bhardwaj, E. Simova, P. P. Rajeev, C. Hnatovsky, R. S. Taylor, D. M. Rayner, and P. B. Corkum, “Optically produced arrays of planar nanostructures inside fused silica,” Phys. Rev. Lett. 96(5), 057404 (2006). [CrossRef] [PubMed]
- D. Emmony, R. Howson, and L. Willis, “Laser mirror damage in germanium at 10.6 µm,” Appl. Phys. Lett. 23(11), 598 (1973). [CrossRef]
- E. Hsu, T. Crawford, C. Maunders, G. Botton, and H. Haugen, “Cross-sectional study of periodic surface structures on gallium phosphide induced by ultrashort laser pulse irradiation,” Appl. Phys. Lett. 92(22), 221112 (2008). [CrossRef]
- M. Huang, F. L. Zhao, Y. Cheng, N. S. Xu, and Z. Z. Xu, “Large area uniform nanostructures fabricated by direct femtosecond laser ablation,” Opt. Express 16(23), 19354–19365 (2008). [CrossRef]
- M. Huang, F. L. Zhao, T. Q. Jia, Y. Cheng, N. S. Xu, and Z. Z. Xu, “A uniform 290 nm periodic square structure on ZnO fabricated by two-beam femtosecond laser ablation,” Nanotechnology 18(50), 505301 (2007). [CrossRef]
- T. Q. Jia, H. X. Chen, M. Huang, F. L. Zhao, X. X. Li,, S. Z. Xu, H. Y. Sun, D. H. Feng, C. B. Li, X. F. Wang, R. X. Li, Z. Z. Xu, X. K. He, and H. Kuroda, “Ultraviolet-infrared femtosecond laser-induced damage in fused silica and CaF2 crystals,” Phys. Rev. B 73(5), 054105 (2006). [CrossRef]
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- T. Q. Jia, M. Baba, M. Suzuki, R. A. Ganeev, H. Kuroda, J. R. Qiu, X. Wang, R. Li, and Z. Xu, “Fabrication of two-dimensional periodic nanostructures by two-beam interference of femtosecond pulses,” Opt. Express 16(3), 1874–1878 (2008). [CrossRef] [PubMed]
- M. Huang, F. L. Zhao, T. Q. Jia, Y. Cheng, N. S. Xu, and Z. Z. Xu, “A uniform 290 nm periodic square structure on ZnO fabricated by two-beam femtosecond laser ablation,” Nanotechnology 18(50), 505301 (2007). [CrossRef]
- T. Q. Jia, H. X. Chen, M. Huang, F. L. Zhao, X. X. Li,, S. Z. Xu, H. Y. Sun, D. H. Feng, C. B. Li, X. F. Wang, R. X. Li, Z. Z. Xu, X. K. He, and H. Kuroda, “Ultraviolet-infrared femtosecond laser-induced damage in fused silica and CaF2 crystals,” Phys. Rev. B 73(5), 054105 (2006). [CrossRef]
- H. Iwase, S. Kokubo, S. Juodkazis, and H. Misawa, “Suppression of ripples on ablated Ni surface via a polarization grating,” Opt. Express 17(6), 4388–4396 (2009). [CrossRef] [PubMed]
- S. Juodkazis, K. Nishimura, and H. Misawa, “In-bulk and surface structuring of sapphire by femtosecond pulses,” Appl. Surf. Sci. 253(15), 6539–6544 (2007). [CrossRef]
- M. Shen, J. E. Carey, C. H. Crouch, M. Kandyla, H. A. Stone, and E. Mazur, “High-density regular arrays of nanometer-scale rods formed on silicon surfaces via femtosecond laser irradiation in water,” Nano Lett. 8(7), 2087–2091 (2008). [CrossRef] [PubMed]
- C. Wu, C. H. Crouch, L. Zhao, J. E. Carey, R. Younkin, J. A. Levinson, E. Mazur, R. M. Farrell, P. Gothoskar, and A. Karger, “Near-unity below-band-gap absorption by microstructured silicon,” Appl. Phys. Lett. 78(13), 1850 (2001). [CrossRef]
- Y. Shimotsuma, P. G. Kazansky, J. R. Qiu, and K. Hirao, “Self-organized nanogratings in glass irradiated by ultrashort light pulses,” Phys. Rev. Lett. 91(24), 247405 (2003). [CrossRef] [PubMed]
- N. Yasumaru, K. Miyazaki, and J. Kiuchi, “Femtosecond-laser-induced nanostructure formed on hard thin film of TiN and DLC,” Appl. Phys., A Mater. Sci. Process. 76(6), 983–985 (2003). [CrossRef]
- T. Q. Jia, M. Baba, M. Suzuki, R. A. Ganeev, H. Kuroda, J. R. Qiu, X. Wang, R. Li, and Z. Xu, “Fabrication of two-dimensional periodic nanostructures by two-beam interference of femtosecond pulses,” Opt. Express 16(3), 1874–1878 (2008). [CrossRef] [PubMed]
- T. Q. Jia, H. X. Chen, M. Huang, F. L. Zhao, X. X. Li,, S. Z. Xu, H. Y. Sun, D. H. Feng, C. B. Li, X. F. Wang, R. X. Li, Z. Z. Xu, X. K. He, and H. Kuroda, “Ultraviolet-infrared femtosecond laser-induced damage in fused silica and CaF2 crystals,” Phys. Rev. B 73(5), 054105 (2006). [CrossRef]
- C. Wu, C. H. Crouch, L. Zhao, J. E. Carey, R. Younkin, J. A. Levinson, E. Mazur, R. M. Farrell, P. Gothoskar, and A. Karger, “Near-unity below-band-gap absorption by microstructured silicon,” Appl. Phys. Lett. 78(13), 1850 (2001). [CrossRef]
- T. Q. Jia, H. X. Chen, M. Huang, F. L. Zhao, X. X. Li,, S. Z. Xu, H. Y. Sun, D. H. Feng, C. B. Li, X. F. Wang, R. X. Li, Z. Z. Xu, X. K. He, and H. Kuroda, “Ultraviolet-infrared femtosecond laser-induced damage in fused silica and CaF2 crystals,” Phys. Rev. B 73(5), 054105 (2006). [CrossRef]
- X. D. Guo, R. X. Li, Y. Hang, Z. Z. Xu, B. K. Yu, Y. Dai, B. Lu, and X. W. Sun, “Coherent linking of periodic nano-ripples on a ZnO crystal surface induced by femtosecond laser pulses,” Appl. Phys., A Mater. Sci. Process. 94(2), 423–426 (2009). [CrossRef]
- X. D. Guo, R. X. Li, Y. Hang, Z. Z. Xu, B. K. Yu, H. L. Ma, B. Lu, and X. W. Sun, “Femtosecond laser-induced periodic surface structure on ZnO,” Mater. Lett. 62(12-13), 1769–1771 (2008). [CrossRef]
- X. D. Guo, R. X. Li, Y. Hang, Z. Z. Xu, B. K. Yu, H. L. Ma, and X. W. Sun, “Raman spectroscopy and luminescent properties of ZnO nanostructures fabricated by femtosecond laser pulses,” Mater. Lett. 61(23-24), 4583–4586 (2007). [CrossRef]
- T. Q. Jia, H. X. Chen, M. Huang, F. L. Zhao, X. X. Li,, S. Z. Xu, H. Y. Sun, D. H. Feng, C. B. Li, X. F. Wang, R. X. Li, Z. Z. Xu, X. K. He, and H. Kuroda, “Ultraviolet-infrared femtosecond laser-induced damage in fused silica and CaF2 crystals,” Phys. Rev. B 73(5), 054105 (2006). [CrossRef]
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- X. D. Guo, R. X. Li, Y. Hang, Z. Z. Xu, B. K. Yu, H. L. Ma, B. Lu, and X. W. Sun, “Femtosecond laser-induced periodic surface structure on ZnO,” Mater. Lett. 62(12-13), 1769–1771 (2008). [CrossRef]
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- X. D. Guo, R. X. Li, Y. Hang, Z. Z. Xu, B. K. Yu, H. L. Ma, and X. W. Sun, “Raman spectroscopy and luminescent properties of ZnO nanostructures fabricated by femtosecond laser pulses,” Mater. Lett. 61(23-24), 4583–4586 (2007). [CrossRef]
- A. S. Mahmood, M. Sivakumar, K. Venkatakrishnan, and B. Tan, “Enhancement of optical absorption of silicon fibrous nanostructure produced using femtosecond laser ablation,” Appl. Phys. Lett. 95(3), 034107 (2009). [CrossRef]
- Q. Z. Zhao, F. Ciobanu, S. Malzer, and L. J. Wang, “Enhancement of optical absorption and photocurrent of 6H-SiC by laser surface nanostructuring,” Appl. Phys. Lett. 91(12), 121107 (2007). [CrossRef]
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- M. Shen, J. E. Carey, C. H. Crouch, M. Kandyla, H. A. Stone, and E. Mazur, “High-density regular arrays of nanometer-scale rods formed on silicon surfaces via femtosecond laser irradiation in water,” Nano Lett. 8(7), 2087–2091 (2008). [CrossRef] [PubMed]
- C. Wu, C. H. Crouch, L. Zhao, J. E. Carey, R. Younkin, J. A. Levinson, E. Mazur, R. M. Farrell, P. Gothoskar, and A. Karger, “Near-unity below-band-gap absorption by microstructured silicon,” Appl. Phys. Lett. 78(13), 1850 (2001). [CrossRef]
- H. Iwase, S. Kokubo, S. Juodkazis, and H. Misawa, “Suppression of ripples on ablated Ni surface via a polarization grating,” Opt. Express 17(6), 4388–4396 (2009). [CrossRef] [PubMed]
- S. Juodkazis, K. Nishimura, and H. Misawa, “In-bulk and surface structuring of sapphire by femtosecond pulses,” Appl. Surf. Sci. 253(15), 6539–6544 (2007). [CrossRef]
- G. Miyaji and K. Miyazaki, “Origin of periodicity in nanostructuring on thin film surfaces ablated with femtosecond laser pulses,” Opt. Express 16(20), 16265–16271 (2008). [CrossRef] [PubMed]
- N. Yasumaru, K. Miyazaki, and J. Kiuchi, “Femtosecond-laser-induced nanostructure formed on hard thin film of TiN and DLC,” Appl. Phys., A Mater. Sci. Process. 76(6), 983–985 (2003). [CrossRef]
- Ü. Özgür, Ya. I. Alivov, C. Liu, A. Teke, M. A. Reshchikov, S. Doğan, V. Avrutin, S.-J. Cho, and H. Morkoç, “A comprehensive review of ZnO materials and devices,” J. Appl. Phys. 98(4), 041301 (2005). [CrossRef]
- J. Bonse, M. Munz, and H. Sturm, “Structure formation on the surface of indium phosphide irradiated by femtosecond laser pulses,” J. Appl. Phys. 97(1), 013538 (2005). [CrossRef]
- S. Juodkazis, K. Nishimura, and H. Misawa, “In-bulk and surface structuring of sapphire by femtosecond pulses,” Appl. Surf. Sci. 253(15), 6539–6544 (2007). [CrossRef]
- Ü. Özgür, Ya. I. Alivov, C. Liu, A. Teke, M. A. Reshchikov, S. Doğan, V. Avrutin, S.-J. Cho, and H. Morkoç, “A comprehensive review of ZnO materials and devices,” J. Appl. Phys. 98(4), 041301 (2005). [CrossRef]
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- X. Jia, T. Q. Jia, L. E. Ding, P. X. Xiong, L. Deng, Z. R. Sun, Z. G. Wang, J. R. Qiu, and Z. Z. Xu, “Complex periodic micro/nanostructures on 6H-SiC crystal induced by the interference of three femtosecond laser beams,” Opt. Lett. 34(6), 788–790 (2009). [CrossRef] [PubMed]
- T. Q. Jia, M. Baba, M. Suzuki, R. A. Ganeev, H. Kuroda, J. R. Qiu, X. Wang, R. Li, and Z. Xu, “Fabrication of two-dimensional periodic nanostructures by two-beam interference of femtosecond pulses,” Opt. Express 16(3), 1874–1878 (2008). [CrossRef] [PubMed]
- Y. Shimotsuma, P. G. Kazansky, J. R. Qiu, and K. Hirao, “Self-organized nanogratings in glass irradiated by ultrashort light pulses,” Phys. Rev. Lett. 91(24), 247405 (2003). [CrossRef] [PubMed]
- V. R. Bhardwaj, E. Simova, P. P. Rajeev, C. Hnatovsky, R. S. Taylor, D. M. Rayner, and P. B. Corkum, “Optically produced arrays of planar nanostructures inside fused silica,” Phys. Rev. Lett. 96(5), 057404 (2006). [CrossRef] [PubMed]
- V. R. Bhardwaj, E. Simova, P. P. Rajeev, C. Hnatovsky, R. S. Taylor, D. M. Rayner, and P. B. Corkum, “Optically produced arrays of planar nanostructures inside fused silica,” Phys. Rev. Lett. 96(5), 057404 (2006). [CrossRef] [PubMed]
- F. Costache, M. Henyk, and J. Reif, “Modification of dielectric surfaces with ultra-short laser pulses,” Appl. Surf. Sci. 186(1-4), 352–357 (2002). [CrossRef]
- Ü. Özgür, Ya. I. Alivov, C. Liu, A. Teke, M. A. Reshchikov, S. Doğan, V. Avrutin, S.-J. Cho, and H. Morkoç, “A comprehensive review of ZnO materials and devices,” J. Appl. Phys. 98(4), 041301 (2005). [CrossRef]
- D. Dufft, A. Rosenfeld, S. K. Das, R. Grunwald, and J. Bonse, “Femtosecond laser-induced periodic surface structures revisited: A comparative study on ZnO,” J. Appl. Phys. 105(3), 034908 (2009). [CrossRef]
- M. Shen, J. E. Carey, C. H. Crouch, M. Kandyla, H. A. Stone, and E. Mazur, “High-density regular arrays of nanometer-scale rods formed on silicon surfaces via femtosecond laser irradiation in water,” Nano Lett. 8(7), 2087–2091 (2008). [CrossRef] [PubMed]
- Y. Shimotsuma, P. G. Kazansky, J. R. Qiu, and K. Hirao, “Self-organized nanogratings in glass irradiated by ultrashort light pulses,” Phys. Rev. Lett. 91(24), 247405 (2003). [CrossRef] [PubMed]
- V. R. Bhardwaj, E. Simova, P. P. Rajeev, C. Hnatovsky, R. S. Taylor, D. M. Rayner, and P. B. Corkum, “Optically produced arrays of planar nanostructures inside fused silica,” Phys. Rev. Lett. 96(5), 057404 (2006). [CrossRef] [PubMed]
- J. F. Young, J. S. Preston, H. M. van Driel, and J. E. Sipe, “Laser-induced periodic surface structure. II. Experiments on Ge, Si, Al, and brass,” Phys. Rev. B 27(2), 1155–1172 (1983). [CrossRef]
- A. S. Mahmood, M. Sivakumar, K. Venkatakrishnan, and B. Tan, “Enhancement of optical absorption of silicon fibrous nanostructure produced using femtosecond laser ablation,” Appl. Phys. Lett. 95(3), 034107 (2009). [CrossRef]
- M. Shen, J. E. Carey, C. H. Crouch, M. Kandyla, H. A. Stone, and E. Mazur, “High-density regular arrays of nanometer-scale rods formed on silicon surfaces via femtosecond laser irradiation in water,” Nano Lett. 8(7), 2087–2091 (2008). [CrossRef] [PubMed]
- J. Bonse, M. Munz, and H. Sturm, “Structure formation on the surface of indium phosphide irradiated by femtosecond laser pulses,” J. Appl. Phys. 97(1), 013538 (2005). [CrossRef]
- T. Q. Jia, H. X. Chen, M. Huang, F. L. Zhao, X. X. Li,, S. Z. Xu, H. Y. Sun, D. H. Feng, C. B. Li, X. F. Wang, R. X. Li, Z. Z. Xu, X. K. He, and H. Kuroda, “Ultraviolet-infrared femtosecond laser-induced damage in fused silica and CaF2 crystals,” Phys. Rev. B 73(5), 054105 (2006). [CrossRef]
- X. D. Guo, R. X. Li, Y. Hang, Z. Z. Xu, B. K. Yu, Y. Dai, B. Lu, and X. W. Sun, “Coherent linking of periodic nano-ripples on a ZnO crystal surface induced by femtosecond laser pulses,” Appl. Phys., A Mater. Sci. Process. 94(2), 423–426 (2009). [CrossRef]
- X. D. Guo, R. X. Li, Y. Hang, Z. Z. Xu, B. K. Yu, H. L. Ma, B. Lu, and X. W. Sun, “Femtosecond laser-induced periodic surface structure on ZnO,” Mater. Lett. 62(12-13), 1769–1771 (2008). [CrossRef]
- X. D. Guo, R. X. Li, Y. Hang, Z. Z. Xu, B. K. Yu, H. L. Ma, and X. W. Sun, “Raman spectroscopy and luminescent properties of ZnO nanostructures fabricated by femtosecond laser pulses,” Mater. Lett. 61(23-24), 4583–4586 (2007). [CrossRef]
- A. S. Mahmood, M. Sivakumar, K. Venkatakrishnan, and B. Tan, “Enhancement of optical absorption of silicon fibrous nanostructure produced using femtosecond laser ablation,” Appl. Phys. Lett. 95(3), 034107 (2009). [CrossRef]
- V. R. Bhardwaj, E. Simova, P. P. Rajeev, C. Hnatovsky, R. S. Taylor, D. M. Rayner, and P. B. Corkum, “Optically produced arrays of planar nanostructures inside fused silica,” Phys. Rev. Lett. 96(5), 057404 (2006). [CrossRef] [PubMed]
- Ü. Özgür, Ya. I. Alivov, C. Liu, A. Teke, M. A. Reshchikov, S. Doğan, V. Avrutin, S.-J. Cho, and H. Morkoç, “A comprehensive review of ZnO materials and devices,” J. Appl. Phys. 98(4), 041301 (2005). [CrossRef]
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- A. S. Mahmood, M. Sivakumar, K. Venkatakrishnan, and B. Tan, “Enhancement of optical absorption of silicon fibrous nanostructure produced using femtosecond laser ablation,” Appl. Phys. Lett. 95(3), 034107 (2009). [CrossRef]
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- M. Huang, F. L. Zhao, Y. Cheng, N. S. Xu, and Z. Z. Xu, “Large area uniform nanostructures fabricated by direct femtosecond laser ablation,” Opt. Express 16(23), 19354–19365 (2008). [CrossRef]
- M. Huang, F. L. Zhao, T. Q. Jia, Y. Cheng, N. S. Xu, and Z. Z. Xu, “A uniform 290 nm periodic square structure on ZnO fabricated by two-beam femtosecond laser ablation,” Nanotechnology 18(50), 505301 (2007). [CrossRef]
- T. Q. Jia, H. X. Chen, M. Huang, F. L. Zhao, X. X. Li,, S. Z. Xu, H. Y. Sun, D. H. Feng, C. B. Li, X. F. Wang, R. X. Li, Z. Z. Xu, X. K. He, and H. Kuroda, “Ultraviolet-infrared femtosecond laser-induced damage in fused silica and CaF2 crystals,” Phys. Rev. B 73(5), 054105 (2006). [CrossRef]
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- M. Huang, F. L. Zhao, Y. Cheng, N. S. Xu, and Z. Z. Xu, “Large area uniform nanostructures fabricated by direct femtosecond laser ablation,” Opt. Express 16(23), 19354–19365 (2008). [CrossRef]
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- X. D. Guo, R. X. Li, Y. Hang, Z. Z. Xu, B. K. Yu, H. L. Ma, B. Lu, and X. W. Sun, “Femtosecond laser-induced periodic surface structure on ZnO,” Mater. Lett. 62(12-13), 1769–1771 (2008). [CrossRef]
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- M. Huang, F. L. Zhao, Y. Cheng, N. S. Xu, and Z. Z. Xu, “Large area uniform nanostructures fabricated by direct femtosecond laser ablation,” Opt. Express 16(23), 19354–19365 (2008). [CrossRef]
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Appl. Phys. Lett.
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Appl. Phys., A Mater. Sci. Process.
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Appl. Surf. Sci.
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Nano Lett.
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Nanotechnology
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Opt. Express
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Opt. Lett.
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