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The rotating-crystal method in femtosecond X-ray diffractionB. Freyer, J. Stingl, F. Zamponi, M. Woerner, and T. Elsaesser »View Author Affiliations
B. Freyer,*
J. Stingl,
F. Zamponi,
M. Woerner,
and T. Elsaesser
Max-Born-Institut für Nichtlineare Optik und Kurzzeitspektroskopie, 12489 Berlin, Germany *Corresponding author: bfreyer@mbi-berlin.de |
Optics Express, Vol. 19, Issue 16, pp. 15506-15515 (2011)
http://dx.doi.org/10.1364/OE.19.015506
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Abstract
We report the first implementation of the rotating-crystal method in femtosecond X-ray diffraction. Applying a pump-probe scheme with 100 fs hard X-ray probe pulses from a laser-driven plasma source, the novel technique is demonstrated by mapping structural dynamics of a photoexcited bismuth crystal via changes of the diffracted intensity on a multitude of Bragg reflections. The method is compared to femtosecond powder diffraction and to Bragg diffraction from a crystal with stationary orientation.
© 2011 OSA
OCIS Codes
(000.2170) General : Equipment and techniques
(320.2250) Ultrafast optics : Femtosecond phenomena
(340.7480) X-ray optics : X-rays, soft x-rays, extreme ultraviolet (EUV)
ToC Category:
X-ray Optics
History
Original Manuscript: May 23, 2011
Revised Manuscript: June 23, 2011
Manuscript Accepted: July 5, 2011
Published: July 28, 2011
Citation
B. Freyer, J. Stingl, F. Zamponi, M. Woerner, and T. Elsaesser, "The rotating-crystal method in femtosecond X-ray diffraction," Opt. Express 19, 15506-15515 (2011)
http://www.opticsinfobase.org/oe/abstract.cfm?URI=oe-19-16-15506
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References
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- F. Zamponi, Z. Ansari, M. Woerner, and T. Elsaesser, “Femtosecond powder diffraction with a laser-driven hard x-ray source,” Opt. Express 18, 947–961 (2010). [CrossRef] [PubMed]
- M. Woerner, F. Zamponi, Z. Ansari, J. Dreyer, B. Freyer, M. Premont-Schwarz, and T. Elsaesser, “Concerted electron and proton transfer in ionic crystals mapped by femtosecond x-ray powder diffraction,” J. Chem. Phys. 133, 064509 (2010). [CrossRef] [PubMed]
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- C. v. Korff Schmising, M. Bargheer, M. Kiel, N. Zhavoronkov, M. Woerner, T. Elsaesser, I. Vrejoiu, D. Hesse, and M. Alexe, “Coupled ultrafast lattice and polarization dynamics in ferroelectric nanolayers,” Phys. Rev. Lett. 98, 257601 (2007). [CrossRef]
- N. Zhavoronkov, Y. Gritsai, M. Bargheer, M. Woerner, Th. Elsaesser, F. Zamponi, I. Uschmann, and E. Förster, “Microfocus Cu Kα source for femtosecond x-ray science,” Opt. Lett. 30, 1737–1739 (2005). [CrossRef] [PubMed]
- M. Bargheer, N. Zhavoronkov, R. Bruch, H. Legall, H. Stiel, M. Woerner, and T. Elsaesser, “Comparison of focusing optics for femtosecond X-ray diffraction,” Appl. Phys. B 80, 715–719 (2005). [CrossRef]
- M. Bargheer, N. Zhavoronkov, Y. Gritsai, J. C. Woo, D. S. Kim, M. Woerner, and T. Elsaesser, “Coherent atomic motions in a nanostructure studied by femtosecond x-ray diffraction,” Science 306, 1771–1773 (2004). [CrossRef] [PubMed]
- S. L. Johnson, P. Beaud, E. Vorobeva, C. J. Milne, É. D. Murray, S. Fahy, and G. Ingold, “Non-equilibrium phonon dynamics studied by grazing-incidence femtosecond X-ray crystallography,” Acta Crystallogr., Sect. A 66, 157–167 (2010). [CrossRef] [PubMed]
- S. L. Johnson, P. Beaud, E. Vorobeva, C. J. Milne, E. D. Murray, S. Fahy, and G. Ingold, “Directly observing squeezed phonon states with femtosecond x-ray diffraction,” Phys. Rev. Lett. 102, 175503 (2009). [CrossRef] [PubMed]
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- D. M. Fritz, D. A. Reis, B. Adams, R. A. Akre, J. Arthur, C. Blome, P. H. Bucksbaum, A. L. Cavalieri, S. Engemann, S. Fahy, R. W. Falcone, P. H. Fuoss, K. J. Gaffney, M. J. George, J. Hajdu, M. P. Hertlein, P. B. Hillyard, M. Horn-von Hoegen, M. Kammler, J. Kaspar, R. Kienberger, P. Krejcik, S. H. Lee, A. M. Lindenberg, B. McFarland, D. Meyer, T. Montagne, A. D. Murray, A. J. Nelson, M. Nicoul, R. Pahl, J. Rudati, H. Schlarb, D. P. Siddons, K. Sokolowski-Tinten, T. Tschentscher, D. von der Linde, and J. B. Hastings, “Ultrafast bond softening in bismuth: mapping a solid’s interatomic potential with x-rays,” Science 315, 633–636 (2007). [CrossRef] [PubMed]
- K. Sokolowski-Tinten, C. Blome, J. Blums, A. Cavalleri, C. Dietrich, A. Tarasevitch, I. Uschmann, E. Förster, M. Kammler, M. Horn-von-Hoegen, and D. von der Linde, “Femtosecond X-ray measurement of coherent lattice vibrations near the Lindemann stability limit,” Nature 422, 287–289 (2003). [CrossRef] [PubMed]
- K. Sokolowski-Tinten, C. Blome, J. Blums, A. Cavalleri, C. Dietrich, A. Tarasevitch, I. Uschmann, E. Förster, M. Kammler, M. Horn-von-Hoegen, and D. von der Linde, “Femtosecond X-ray measurement of coherent lattice vibrations near the Lindemann stability limit,” Nature 422, 287–289 (2003). [CrossRef] [PubMed]
- W. L. Bragg, “The structure of some crystals as indicated by their diffraction of x-rays,” Proc. R. Soc. London, Ser. A 89, 248–277 (1913). [CrossRef]
- M. Bargheer, N. Zhavoronkov, R. Bruch, H. Legall, H. Stiel, M. Woerner, and T. Elsaesser, “Comparison of focusing optics for femtosecond X-ray diffraction,” Appl. Phys. B 80, 715–719 (2005). [CrossRef]
- J. B. Woodhouse, A. L. A. Fields, and I. A. Bucklow, “X-ray mass absorption coefficients for gold, lead and bismuth in the range 1–10 Å,” J. Phys. D: Appl. Phys, 7, 483–489 (1974). [CrossRef]
- D. M. Fritz, D. A. Reis, B. Adams, R. A. Akre, J. Arthur, C. Blome, P. H. Bucksbaum, A. L. Cavalieri, S. Engemann, S. Fahy, R. W. Falcone, P. H. Fuoss, K. J. Gaffney, M. J. George, J. Hajdu, M. P. Hertlein, P. B. Hillyard, M. Horn-von Hoegen, M. Kammler, J. Kaspar, R. Kienberger, P. Krejcik, S. H. Lee, A. M. Lindenberg, B. McFarland, D. Meyer, T. Montagne, A. D. Murray, A. J. Nelson, M. Nicoul, R. Pahl, J. Rudati, H. Schlarb, D. P. Siddons, K. Sokolowski-Tinten, T. Tschentscher, D. von der Linde, and J. B. Hastings, “Ultrafast bond softening in bismuth: mapping a solid’s interatomic potential with x-rays,” Science 315, 633–636 (2007). [CrossRef] [PubMed]
- E. Collet, M.-H. Leme-Cailleau, M. Buron-Le Cointe, H. Cailleau, M. Wulff, T. Luty, S.-Y. Koshihara, M. Meyer, L. Toupet, P. Rabiller, and S. Techert, “Laser-induced ferroelectric structural order in an organic charge-transfer crystal,” Science 300, 612–615 (2003). [CrossRef] [PubMed]
- E. Collet, M.-H. Leme-Cailleau, M. Buron-Le Cointe, H. Cailleau, M. Wulff, T. Luty, S.-Y. Koshihara, M. Meyer, L. Toupet, P. Rabiller, and S. Techert, “Laser-induced ferroelectric structural order in an organic charge-transfer crystal,” Science 300, 612–615 (2003). [CrossRef] [PubMed]
- D. M. Fritz, D. A. Reis, B. Adams, R. A. Akre, J. Arthur, C. Blome, P. H. Bucksbaum, A. L. Cavalieri, S. Engemann, S. Fahy, R. W. Falcone, P. H. Fuoss, K. J. Gaffney, M. J. George, J. Hajdu, M. P. Hertlein, P. B. Hillyard, M. Horn-von Hoegen, M. Kammler, J. Kaspar, R. Kienberger, P. Krejcik, S. H. Lee, A. M. Lindenberg, B. McFarland, D. Meyer, T. Montagne, A. D. Murray, A. J. Nelson, M. Nicoul, R. Pahl, J. Rudati, H. Schlarb, D. P. Siddons, K. Sokolowski-Tinten, T. Tschentscher, D. von der Linde, and J. B. Hastings, “Ultrafast bond softening in bismuth: mapping a solid’s interatomic potential with x-rays,” Science 315, 633–636 (2007). [CrossRef] [PubMed]
- K. Sokolowski-Tinten, C. Blome, J. Blums, A. Cavalleri, C. Dietrich, A. Tarasevitch, I. Uschmann, E. Förster, M. Kammler, M. Horn-von-Hoegen, and D. von der Linde, “Femtosecond X-ray measurement of coherent lattice vibrations near the Lindemann stability limit,” Nature 422, 287–289 (2003). [CrossRef] [PubMed]
- C. Rose-Petruck, R. Jiminez, T. Guo, A. Cavalleri, C. Siders, J. A. Squier, B. C. Walker, and K. R. Wilson, “Picosecond millianstrom lattice dynamics measured by ultrafast x-ray diffraction,” Nature 398, 310–312 (1999). [CrossRef]
- U. W. Arndt, J. N. Champness, R. P. Phizackerley, and A. J. Wonacott, “A single-crystal oscillation camera for large unit cells,” J. Appl. Cryst. 6, 457–463 (1973). [CrossRef]
- E. Collet, M.-H. Leme-Cailleau, M. Buron-Le Cointe, H. Cailleau, M. Wulff, T. Luty, S.-Y. Koshihara, M. Meyer, L. Toupet, P. Rabiller, and S. Techert, “Laser-induced ferroelectric structural order in an organic charge-transfer crystal,” Science 300, 612–615 (2003). [CrossRef] [PubMed]
- K. Sokolowski-Tinten, C. Blome, J. Blums, A. Cavalleri, C. Dietrich, A. Tarasevitch, I. Uschmann, E. Förster, M. Kammler, M. Horn-von-Hoegen, and D. von der Linde, “Femtosecond X-ray measurement of coherent lattice vibrations near the Lindemann stability limit,” Nature 422, 287–289 (2003). [CrossRef] [PubMed]
- M. Woerner, F. Zamponi, Z. Ansari, J. Dreyer, B. Freyer, M. Premont-Schwarz, and T. Elsaesser, “Concerted electron and proton transfer in ionic crystals mapped by femtosecond x-ray powder diffraction,” J. Chem. Phys. 133, 064509 (2010). [CrossRef] [PubMed]
- F. Zamponi, Z. Ansari, M. Woerner, and T. Elsaesser, “Femtosecond powder diffraction with a laser-driven hard x-ray source,” Opt. Express 18, 947–961 (2010). [CrossRef] [PubMed]
- M. Woerner, F. Zamponi, Z. Ansari, J. Dreyer, B. Freyer, M. Premont-Schwarz, and T. Elsaesser, “Concerted electron and proton transfer in ionic crystals mapped by femtosecond x-ray powder diffraction,” J. Chem. Phys. 133, 064509 (2010). [CrossRef] [PubMed]
- T. Elsaesser and M. Woerner, “Photoinduced structural dynamics of polar solids studied by femtosecond x-ray diffraction,” Acta Crystallogr., Sect. A 66, 168–178 (2010). [CrossRef] [PubMed]
- C. v. Korff Schmising, M. Bargheer, M. Kiel, N. Zhavoronkov, M. Woerner, T. Elsaesser, I. Vrejoiu, D. Hesse, and M. Alexe, “Coupled ultrafast lattice and polarization dynamics in ferroelectric nanolayers,” Phys. Rev. Lett. 98, 257601 (2007). [CrossRef]
- M. Bargheer, N. Zhavoronkov, R. Bruch, H. Legall, H. Stiel, M. Woerner, and T. Elsaesser, “Comparison of focusing optics for femtosecond X-ray diffraction,” Appl. Phys. B 80, 715–719 (2005). [CrossRef]
- M. Bargheer, N. Zhavoronkov, Y. Gritsai, J. C. Woo, D. S. Kim, M. Woerner, and T. Elsaesser, “Coherent atomic motions in a nanostructure studied by femtosecond x-ray diffraction,” Science 306, 1771–1773 (2004). [CrossRef] [PubMed]
- D. M. Fritz, D. A. Reis, B. Adams, R. A. Akre, J. Arthur, C. Blome, P. H. Bucksbaum, A. L. Cavalieri, S. Engemann, S. Fahy, R. W. Falcone, P. H. Fuoss, K. J. Gaffney, M. J. George, J. Hajdu, M. P. Hertlein, P. B. Hillyard, M. Horn-von Hoegen, M. Kammler, J. Kaspar, R. Kienberger, P. Krejcik, S. H. Lee, A. M. Lindenberg, B. McFarland, D. Meyer, T. Montagne, A. D. Murray, A. J. Nelson, M. Nicoul, R. Pahl, J. Rudati, H. Schlarb, D. P. Siddons, K. Sokolowski-Tinten, T. Tschentscher, D. von der Linde, and J. B. Hastings, “Ultrafast bond softening in bismuth: mapping a solid’s interatomic potential with x-rays,” Science 315, 633–636 (2007). [CrossRef] [PubMed]
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- B. E. Warren, X-ray Diffraction (Dover Publications, 1990).
- C. Rose-Petruck, R. Jiminez, T. Guo, A. Cavalleri, C. Siders, J. A. Squier, B. C. Walker, and K. R. Wilson, “Picosecond millianstrom lattice dynamics measured by ultrafast x-ray diffraction,” Nature 398, 310–312 (1999). [CrossRef]
- T. Elsaesser and M. Woerner, “Photoinduced structural dynamics of polar solids studied by femtosecond x-ray diffraction,” Acta Crystallogr., Sect. A 66, 168–178 (2010). [CrossRef] [PubMed]
- M. Woerner, F. Zamponi, Z. Ansari, J. Dreyer, B. Freyer, M. Premont-Schwarz, and T. Elsaesser, “Concerted electron and proton transfer in ionic crystals mapped by femtosecond x-ray powder diffraction,” J. Chem. Phys. 133, 064509 (2010). [CrossRef] [PubMed]
- F. Zamponi, Z. Ansari, M. Woerner, and T. Elsaesser, “Femtosecond powder diffraction with a laser-driven hard x-ray source,” Opt. Express 18, 947–961 (2010). [CrossRef] [PubMed]
- C. v. Korff Schmising, M. Bargheer, M. Kiel, N. Zhavoronkov, M. Woerner, T. Elsaesser, I. Vrejoiu, D. Hesse, and M. Alexe, “Coupled ultrafast lattice and polarization dynamics in ferroelectric nanolayers,” Phys. Rev. Lett. 98, 257601 (2007). [CrossRef]
- N. Zhavoronkov, Y. Gritsai, M. Bargheer, M. Woerner, Th. Elsaesser, F. Zamponi, I. Uschmann, and E. Förster, “Microfocus Cu Kα source for femtosecond x-ray science,” Opt. Lett. 30, 1737–1739 (2005). [CrossRef] [PubMed]
- M. Bargheer, N. Zhavoronkov, R. Bruch, H. Legall, H. Stiel, M. Woerner, and T. Elsaesser, “Comparison of focusing optics for femtosecond X-ray diffraction,” Appl. Phys. B 80, 715–719 (2005). [CrossRef]
- M. Bargheer, N. Zhavoronkov, Y. Gritsai, J. C. Woo, D. S. Kim, M. Woerner, and T. Elsaesser, “Coherent atomic motions in a nanostructure studied by femtosecond x-ray diffraction,” Science 306, 1771–1773 (2004). [CrossRef] [PubMed]
- U. W. Arndt, J. N. Champness, R. P. Phizackerley, and A. J. Wonacott, “A single-crystal oscillation camera for large unit cells,” J. Appl. Cryst. 6, 457–463 (1973). [CrossRef]
- M. Bargheer, N. Zhavoronkov, Y. Gritsai, J. C. Woo, D. S. Kim, M. Woerner, and T. Elsaesser, “Coherent atomic motions in a nanostructure studied by femtosecond x-ray diffraction,” Science 306, 1771–1773 (2004). [CrossRef] [PubMed]
- J. B. Woodhouse, A. L. A. Fields, and I. A. Bucklow, “X-ray mass absorption coefficients for gold, lead and bismuth in the range 1–10 Å,” J. Phys. D: Appl. Phys, 7, 483–489 (1974). [CrossRef]
- E. Collet, M.-H. Leme-Cailleau, M. Buron-Le Cointe, H. Cailleau, M. Wulff, T. Luty, S.-Y. Koshihara, M. Meyer, L. Toupet, P. Rabiller, and S. Techert, “Laser-induced ferroelectric structural order in an organic charge-transfer crystal,” Science 300, 612–615 (2003). [CrossRef] [PubMed]
- M. Woerner, F. Zamponi, Z. Ansari, J. Dreyer, B. Freyer, M. Premont-Schwarz, and T. Elsaesser, “Concerted electron and proton transfer in ionic crystals mapped by femtosecond x-ray powder diffraction,” J. Chem. Phys. 133, 064509 (2010). [CrossRef] [PubMed]
- F. Zamponi, Z. Ansari, M. Woerner, and T. Elsaesser, “Femtosecond powder diffraction with a laser-driven hard x-ray source,” Opt. Express 18, 947–961 (2010). [CrossRef] [PubMed]
- N. Zhavoronkov, Y. Gritsai, M. Bargheer, M. Woerner, Th. Elsaesser, F. Zamponi, I. Uschmann, and E. Förster, “Microfocus Cu Kα source for femtosecond x-ray science,” Opt. Lett. 30, 1737–1739 (2005). [CrossRef] [PubMed]
- C. v. Korff Schmising, M. Bargheer, M. Kiel, N. Zhavoronkov, M. Woerner, T. Elsaesser, I. Vrejoiu, D. Hesse, and M. Alexe, “Coupled ultrafast lattice and polarization dynamics in ferroelectric nanolayers,” Phys. Rev. Lett. 98, 257601 (2007). [CrossRef]
- M. Bargheer, N. Zhavoronkov, R. Bruch, H. Legall, H. Stiel, M. Woerner, and T. Elsaesser, “Comparison of focusing optics for femtosecond X-ray diffraction,” Appl. Phys. B 80, 715–719 (2005). [CrossRef]
- N. Zhavoronkov, Y. Gritsai, M. Bargheer, M. Woerner, Th. Elsaesser, F. Zamponi, I. Uschmann, and E. Förster, “Microfocus Cu Kα source for femtosecond x-ray science,” Opt. Lett. 30, 1737–1739 (2005). [CrossRef] [PubMed]
- M. Bargheer, N. Zhavoronkov, Y. Gritsai, J. C. Woo, D. S. Kim, M. Woerner, and T. Elsaesser, “Coherent atomic motions in a nanostructure studied by femtosecond x-ray diffraction,” Science 306, 1771–1773 (2004). [CrossRef] [PubMed]
- S. L. Johnson, P. Beaud, C. J. Milne, F. S. Krasniqi, E. S. Zijlstra, M. E. Garcia, M. Kaiser, D. Grolimund, R. Abela, and G. Ingold, “Nanoscale depth-resolved coherent femtosecond motion in laser-excited bismuth,” Phys. Rev. Lett. 100, 155501 (2008). [CrossRef] [PubMed]
Acta Crystallogr., Sect. A
- E. Colleted., “Dynamical structural science,” Acta Crystallogr., Sect. A 66, 133–280 (2010). [CrossRef] [PubMed]
- T. Elsaesser and M. Woerner, “Photoinduced structural dynamics of polar solids studied by femtosecond x-ray diffraction,” Acta Crystallogr., Sect. A 66, 168–178 (2010). [CrossRef] [PubMed]
- S. L. Johnson, P. Beaud, E. Vorobeva, C. J. Milne, É. D. Murray, S. Fahy, and G. Ingold, “Non-equilibrium phonon dynamics studied by grazing-incidence femtosecond X-ray crystallography,” Acta Crystallogr., Sect. A 66, 157–167 (2010). [CrossRef] [PubMed]
Appl. Phys. B
- M. Bargheer, N. Zhavoronkov, R. Bruch, H. Legall, H. Stiel, M. Woerner, and T. Elsaesser, “Comparison of focusing optics for femtosecond X-ray diffraction,” Appl. Phys. B 80, 715–719 (2005). [CrossRef]
J. Appl. Cryst.
- U. W. Arndt, J. N. Champness, R. P. Phizackerley, and A. J. Wonacott, “A single-crystal oscillation camera for large unit cells,” J. Appl. Cryst. 6, 457–463 (1973). [CrossRef]
J. Chem. Phys.
- M. Woerner, F. Zamponi, Z. Ansari, J. Dreyer, B. Freyer, M. Premont-Schwarz, and T. Elsaesser, “Concerted electron and proton transfer in ionic crystals mapped by femtosecond x-ray powder diffraction,” J. Chem. Phys. 133, 064509 (2010). [CrossRef] [PubMed]
J. Phys. D: Appl. Phys,
- J. B. Woodhouse, A. L. A. Fields, and I. A. Bucklow, “X-ray mass absorption coefficients for gold, lead and bismuth in the range 1–10 Å,” J. Phys. D: Appl. Phys, 7, 483–489 (1974). [CrossRef]
Nature
- C. Rischel, A. Rousse, I. Uschmann, P.-A. Albouy, J.-P. Geindre, P. Audebert, J.-C. Gauthier, E. Forster, J.-L. Martin, and A. Antonetti, “Femtosecond time-resolved X-ray diffraction from laser-heated organic films,” Nature 390, 490–492 (1997). [CrossRef]
- C. Rose-Petruck, R. Jiminez, T. Guo, A. Cavalleri, C. Siders, J. A. Squier, B. C. Walker, and K. R. Wilson, “Picosecond millianstrom lattice dynamics measured by ultrafast x-ray diffraction,” Nature 398, 310–312 (1999). [CrossRef]
- K. Sokolowski-Tinten, C. Blome, J. Blums, A. Cavalleri, C. Dietrich, A. Tarasevitch, I. Uschmann, E. Förster, M. Kammler, M. Horn-von-Hoegen, and D. von der Linde, “Femtosecond X-ray measurement of coherent lattice vibrations near the Lindemann stability limit,” Nature 422, 287–289 (2003). [CrossRef] [PubMed]
Opt. Express
- F. Zamponi, Z. Ansari, M. Woerner, and T. Elsaesser, “Femtosecond powder diffraction with a laser-driven hard x-ray source,” Opt. Express 18, 947–961 (2010). [CrossRef] [PubMed]
Opt. Lett.
- N. Zhavoronkov, Y. Gritsai, M. Bargheer, M. Woerner, Th. Elsaesser, F. Zamponi, I. Uschmann, and E. Förster, “Microfocus Cu Kα source for femtosecond x-ray science,” Opt. Lett. 30, 1737–1739 (2005). [CrossRef] [PubMed]
Phys. Rev. Lett.
- C. v. Korff Schmising, M. Bargheer, M. Kiel, N. Zhavoronkov, M. Woerner, T. Elsaesser, I. Vrejoiu, D. Hesse, and M. Alexe, “Coupled ultrafast lattice and polarization dynamics in ferroelectric nanolayers,” Phys. Rev. Lett. 98, 257601 (2007). [CrossRef]
- S. L. Johnson, P. Beaud, C. J. Milne, F. S. Krasniqi, E. S. Zijlstra, M. E. Garcia, M. Kaiser, D. Grolimund, R. Abela, and G. Ingold, “Nanoscale depth-resolved coherent femtosecond motion in laser-excited bismuth,” Phys. Rev. Lett. 100, 155501 (2008). [CrossRef] [PubMed]
- S. L. Johnson, P. Beaud, E. Vorobeva, C. J. Milne, E. D. Murray, S. Fahy, and G. Ingold, “Directly observing squeezed phonon states with femtosecond x-ray diffraction,” Phys. Rev. Lett. 102, 175503 (2009). [CrossRef] [PubMed]
Proc. R. Soc. London, Ser. A
- W. L. Bragg, “The structure of some crystals as indicated by their diffraction of x-rays,” Proc. R. Soc. London, Ser. A 89, 248–277 (1913). [CrossRef]
Rev. Mod. Phys.
- A. Rousse, C. Rischel, and J. C. Gauthier, “Colloquium: femtosecond x-ray crystallography,” Rev. Mod. Phys. 73, 17–31 (2001). [CrossRef]
Science
- M. Bargheer, N. Zhavoronkov, Y. Gritsai, J. C. Woo, D. S. Kim, M. Woerner, and T. Elsaesser, “Coherent atomic motions in a nanostructure studied by femtosecond x-ray diffraction,” Science 306, 1771–1773 (2004). [CrossRef] [PubMed]
- D. M. Fritz, D. A. Reis, B. Adams, R. A. Akre, J. Arthur, C. Blome, P. H. Bucksbaum, A. L. Cavalieri, S. Engemann, S. Fahy, R. W. Falcone, P. H. Fuoss, K. J. Gaffney, M. J. George, J. Hajdu, M. P. Hertlein, P. B. Hillyard, M. Horn-von Hoegen, M. Kammler, J. Kaspar, R. Kienberger, P. Krejcik, S. H. Lee, A. M. Lindenberg, B. McFarland, D. Meyer, T. Montagne, A. D. Murray, A. J. Nelson, M. Nicoul, R. Pahl, J. Rudati, H. Schlarb, D. P. Siddons, K. Sokolowski-Tinten, T. Tschentscher, D. von der Linde, and J. B. Hastings, “Ultrafast bond softening in bismuth: mapping a solid’s interatomic potential with x-rays,” Science 315, 633–636 (2007). [CrossRef] [PubMed]
- E. Collet, M.-H. Leme-Cailleau, M. Buron-Le Cointe, H. Cailleau, M. Wulff, T. Luty, S.-Y. Koshihara, M. Meyer, L. Toupet, P. Rabiller, and S. Techert, “Laser-induced ferroelectric structural order in an organic charge-transfer crystal,” Science 300, 612–615 (2003). [CrossRef] [PubMed]
Other
- B. E. Warren, X-ray Diffraction (Dover Publications, 1990).
- C. Giacovazzo, Fundamentals of Crystallography (Oxford University Press, 2002). [PubMed]
- L. D. Landau, E. M. Lifshitz, and L. P. Pitaevskii, Electrodynamics of Continuous Media , 2nd ed. (Butterworth-Heinenann, 1984).
- It is important to note that the experimentally observed damage does not change the X-ray diffraction pattern, i.e., the crystal structure, but the surface quality of the single crystal and, thus, the coupling of the optical pump beam into the crystal.
- W. Lu, M. Nicoul, U. Shymanovich, A. Tarasevitch, M. Kammler, M. Horn von Hoegen, D. von der Linde, and K. Sokolowski-Tinten, “Transient reversal of a Peierls-transition: Extreme phonon softening in laser-excited Bismuth,” in Ultrafast Phenomena XVII , M. Chergui, D. Jonas, E. Riedle, R. Schoenlein, and A. Taylor, eds. (Oxford University Press, 2011).
2010, , Acta Crystallogr., Sect. A
- E. Colleted., “Dynamical structural science,” Acta Crystallogr., Sect. A 66, 133–280 (2010). [CrossRef] [PubMed]
- T. Elsaesser and M. Woerner, “Photoinduced structural dynamics of polar solids studied by femtosecond x-ray diffraction,” Acta Crystallogr., Sect. A 66, 168–178 (2010). [CrossRef] [PubMed]
- M. Woerner, F. Zamponi, Z. Ansari, J. Dreyer, B. Freyer, M. Premont-Schwarz, and T. Elsaesser, “Concerted electron and proton transfer in ionic crystals mapped by femtosecond x-ray powder diffraction,” J. Chem. Phys. 133, 064509 (2010). [CrossRef] [PubMed]
- S. L. Johnson, P. Beaud, E. Vorobeva, C. J. Milne, É. D. Murray, S. Fahy, and G. Ingold, “Non-equilibrium phonon dynamics studied by grazing-incidence femtosecond X-ray crystallography,” Acta Crystallogr., Sect. A 66, 157–167 (2010). [CrossRef] [PubMed]
- S. L. Johnson, P. Beaud, E. Vorobeva, C. J. Milne, E. D. Murray, S. Fahy, and G. Ingold, “Directly observing squeezed phonon states with femtosecond x-ray diffraction,” Phys. Rev. Lett. 102, 175503 (2009). [CrossRef] [PubMed]
- S. L. Johnson, P. Beaud, C. J. Milne, F. S. Krasniqi, E. S. Zijlstra, M. E. Garcia, M. Kaiser, D. Grolimund, R. Abela, and G. Ingold, “Nanoscale depth-resolved coherent femtosecond motion in laser-excited bismuth,” Phys. Rev. Lett. 100, 155501 (2008). [CrossRef] [PubMed]
- D. M. Fritz, D. A. Reis, B. Adams, R. A. Akre, J. Arthur, C. Blome, P. H. Bucksbaum, A. L. Cavalieri, S. Engemann, S. Fahy, R. W. Falcone, P. H. Fuoss, K. J. Gaffney, M. J. George, J. Hajdu, M. P. Hertlein, P. B. Hillyard, M. Horn-von Hoegen, M. Kammler, J. Kaspar, R. Kienberger, P. Krejcik, S. H. Lee, A. M. Lindenberg, B. McFarland, D. Meyer, T. Montagne, A. D. Murray, A. J. Nelson, M. Nicoul, R. Pahl, J. Rudati, H. Schlarb, D. P. Siddons, K. Sokolowski-Tinten, T. Tschentscher, D. von der Linde, and J. B. Hastings, “Ultrafast bond softening in bismuth: mapping a solid’s interatomic potential with x-rays,” Science 315, 633–636 (2007). [CrossRef] [PubMed]
- C. v. Korff Schmising, M. Bargheer, M. Kiel, N. Zhavoronkov, M. Woerner, T. Elsaesser, I. Vrejoiu, D. Hesse, and M. Alexe, “Coupled ultrafast lattice and polarization dynamics in ferroelectric nanolayers,” Phys. Rev. Lett. 98, 257601 (2007). [CrossRef]
- M. Bargheer, N. Zhavoronkov, R. Bruch, H. Legall, H. Stiel, M. Woerner, and T. Elsaesser, “Comparison of focusing optics for femtosecond X-ray diffraction,” Appl. Phys. B 80, 715–719 (2005). [CrossRef]
- M. Bargheer, N. Zhavoronkov, Y. Gritsai, J. C. Woo, D. S. Kim, M. Woerner, and T. Elsaesser, “Coherent atomic motions in a nanostructure studied by femtosecond x-ray diffraction,” Science 306, 1771–1773 (2004). [CrossRef] [PubMed]
- E. Collet, M.-H. Leme-Cailleau, M. Buron-Le Cointe, H. Cailleau, M. Wulff, T. Luty, S.-Y. Koshihara, M. Meyer, L. Toupet, P. Rabiller, and S. Techert, “Laser-induced ferroelectric structural order in an organic charge-transfer crystal,” Science 300, 612–615 (2003). [CrossRef] [PubMed]
- K. Sokolowski-Tinten, C. Blome, J. Blums, A. Cavalleri, C. Dietrich, A. Tarasevitch, I. Uschmann, E. Förster, M. Kammler, M. Horn-von-Hoegen, and D. von der Linde, “Femtosecond X-ray measurement of coherent lattice vibrations near the Lindemann stability limit,” Nature 422, 287–289 (2003). [CrossRef] [PubMed]
- A. Rousse, C. Rischel, and J. C. Gauthier, “Colloquium: femtosecond x-ray crystallography,” Rev. Mod. Phys. 73, 17–31 (2001). [CrossRef]
- C. Rose-Petruck, R. Jiminez, T. Guo, A. Cavalleri, C. Siders, J. A. Squier, B. C. Walker, and K. R. Wilson, “Picosecond millianstrom lattice dynamics measured by ultrafast x-ray diffraction,” Nature 398, 310–312 (1999). [CrossRef]
- C. Rischel, A. Rousse, I. Uschmann, P.-A. Albouy, J.-P. Geindre, P. Audebert, J.-C. Gauthier, E. Forster, J.-L. Martin, and A. Antonetti, “Femtosecond time-resolved X-ray diffraction from laser-heated organic films,” Nature 390, 490–492 (1997). [CrossRef]
- J. B. Woodhouse, A. L. A. Fields, and I. A. Bucklow, “X-ray mass absorption coefficients for gold, lead and bismuth in the range 1–10 Å,” J. Phys. D: Appl. Phys, 7, 483–489 (1974). [CrossRef]
- U. W. Arndt, J. N. Champness, R. P. Phizackerley, and A. J. Wonacott, “A single-crystal oscillation camera for large unit cells,” J. Appl. Cryst. 6, 457–463 (1973). [CrossRef]
- W. L. Bragg, “The structure of some crystals as indicated by their diffraction of x-rays,” Proc. R. Soc. London, Ser. A 89, 248–277 (1913). [CrossRef]
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