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Optics Express

Optics Express

  • Editor: Andrew M. Weiner
  • Vol. 21, Iss. 23 — Nov. 18, 2013
  • pp: 28019–28028

Using coherent X-ray ptychography to probe medium-range order

A. T. J. Torrance, B. Abbey, C. T. Putkunz, D. Pelliccia, E. Balaur, G. J. Williams, D. J. Vine, A. Y. Nikulin, I. McNulty, H. M. Quiney, and K. A. Nugent  »View Author Affiliations


Optics Express, Vol. 21, Issue 23, pp. 28019-28028 (2013)
http://dx.doi.org/10.1364/OE.21.028019


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Abstract

Characterization of microscopic structural order and in particular medium range order (MRO) in amorphous materials is challenging. A new technique is demonstrated that allows analysis of MRO using X-rays. Diffraction data were collected from a sample consisting of densely packed polystyrene-latex micro-spheres. Ptychography is used to reconstruct the sample transmission function and fluctuation microscopy applied to characterize structural order producing a detailed `fluctuation map' allowing analysis of the sample at two distinct length scales. Independent verification is provided via X-ray diffractometry. Simulations of dense random packing of spheres have also been used to explore the origin of the structural order measured.

© 2013 Optical Society of America

OCIS Codes
(160.2750) Materials : Glass and other amorphous materials
(180.7460) Microscopy : X-ray microscopy

ToC Category:
Microscopy

History
Original Manuscript: September 9, 2013
Revised Manuscript: October 26, 2013
Manuscript Accepted: October 28, 2013
Published: November 7, 2013

Virtual Issues
Vol. 9, Iss. 1 Virtual Journal for Biomedical Optics

Citation
A. T. J. Torrance, B. Abbey, C. T. Putkunz, D. Pelliccia, E. Balaur, G. J. Williams, D. J. Vine, A. Y. Nikulin, I. McNulty, H. M. Quiney, and K. A. Nugent, "Using coherent X-ray ptychography to probe medium-range order," Opt. Express 21, 28019-28028 (2013)
http://www.opticsinfobase.org/oe/abstract.cfm?URI=oe-21-23-28019


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